US 12454464 B1Patent grantUnited States

Porous Titanate-Carbon Water-Treatment Material

Official patent title

Calcium titanate/magnesium titanate/carbon-based nanocomposite

Arabic title: مركب نانوي قائم على تيتانات الكالسيوم/تيتانات المغنيسيوم/الكربون

Invention

Invention

Problem

Titanium-based nanocomposites can have non-uniform phase distribution, uncontrolled particle or crystallite size, inadequate porosity, agglomeration, high energy demand, lengthy processing, or scalability limitations.

Why it matters

A defined porous three-component material could support catalytic or environmental research, but target-specific performance, stability, leaching, reuse, and scalable manufacture require independent validation.

Approach

The patent forms a gel from calcium and magnesium salts, a titanium alkoxide, and a polyol, then dries and calcines it to produce carbon with CaTiO3 and MgTiO3 crystalline phases.

Who may benefit

Potential beneficiaries include titanate-material laboratories, catalyst and adsorbent researchers, environmental-remediation groups, specialty-ceramic manufacturers, and process developers studying multiphase porous powders.

Potential value

The disclosure connects two specified titanate phases and carbon with elemental ranges, heterogeneous particle and pore features, and a bounded gel, drying, and calcination process.

Background

Background

Titanium-oxide and titanate materials are investigated for catalysis, energy storage, and electronic or environmental applications. Single-phase and binary materials may not provide the desired combination of structural stability, porosity, and multifunctionality. Hydrothermal, sol-gel, and solid-state routes can also produce uneven phase distribution, uncontrolled size, inadequate pores, or high energy demand. The patent proposes a carbon-containing calcium-titanate/magnesium-titanate composite and defines its phase identity, elemental composition, crystallite size, morphology, pore fractions, and production sequence.

Technology overview

Technology overview

XRD identifies carbon, orthorhombic CaTiO3, and rhombohedral MgTiO3. Claim 1 specifies about 1–5 at.% C, 20–35 at.% Ti, 5–15 at.% Mg, and 5–15 at.% Ca. Calcium and magnesium salts are added to a titanium-compound solution in a polar protic solvent, and a polyol forms a gel. The gel is heated at about 100–200 °C to a dry powder and calcined at about 600–800 °C. The product includes spherical, flake-like, and agglomerated particles with heterogeneous pores.

Potential applications

Potential applications

  1. Potential immobilization studies for inorganic aqueous pollutants.
  2. Potential actinic-light degradation studies for organic pollutants.
  3. Potential catalyst or adsorbent material research.
  4. Potential multiphase titanate process-development studies.

Evidence-supported advantages

Evidence-supported advantages

  1. Combines carbon with two defined titanate phases.
  2. Specifies elemental and crystallite-size ranges.
  3. Defines multiple particle shapes and two pore fractions.
  4. Provides a corresponding gel and calcination method.

Development stage

Development stage

Patent publication describing material synthesis and characterization; independent application performance and commercialization were not established.

Commercial opportunity

Commercial opportunity

The material may interest specialty-ceramic, catalyst, adsorbent, or environmental-technology developers. Commercial assessment should establish phase and pore reproducibility, batch consistency, contaminant-specific capacity or catalytic rates, stability and reuse, constituent leaching, treated-medium safety, scale-up of gel handling and calcination, energy consumption, product-form integration, and comparative cost.

Patent classifications

Patent classifications

WIPO IPC

  • C01G23/00Compounds containing metals not covered by subclasses C01D or C01F
  • B82Y30/00Specific uses or applications of nanostructures; measurement or analysis of nanostructures; manufacture or treatment of nanostructures

CPC

  • C01G23/006Compounds containing metals not covered by subclasses C01D or C01F
  • B82Y30/00Specific uses or applications of nanostructures; measurement or analysis of nanostructures; manufacture or treatment of nanostructures
  • C01G23/005Compounds containing metals not covered by subclasses C01D or C01F
  • C01P2006/16Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2002/76Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2004/64Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2002/60Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2004/50Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2004/03Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2004/32Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2002/85Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2004/80Indexing scheme for structural and physical aspects of solid inorganic compounds
  • C01P2004/04Indexing scheme for structural and physical aspects of solid inorganic compounds

Inventors

Inventors

  • First inventorEhab Abdelhamed Abdelrahman Ahmed
  • InventorBabiker Yagoub Elhadi Abdulkhair

Keywords

Keywords

  • CaTiO3
  • MgTiO3
  • carbon
  • porous nanocomposite
  • titanate
  • sol-gel
  • calcination
  • water remediation

Patent document and drawings

Patent document and drawings

The patent publication is mapped to this record. Patent drawings remain within that publication; no separately cleared public media package has been supplied.